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References

2012

Articles:

Peresvochchikova, N., Appolaire, B., Teixeira, J., Aeby-Gautier, E. and Denis, S.
Computational Material Science, 61:54--66
2012

Equipe: Département SI2M : Microstructures et Contraintes

Brunetti, G., Settefrati, A., Hazotte, A., Denis, S., Fundenberger, J. -J., Tidu, A. and Bouzy, E.
Micron, 43(2-3):396-406
2012
ISSN: 0968-4328

Resume: In single-crystal nickel-based superalloys, the lattice mismatch associated with interface coherency between gamma matrix and gamma' precipitates has a strong influence on mechanical properties. The unconstrained lattice misfit in a single-crystal of the MC2 nickel-based superalloy is determined using convergent beam electron diffraction measurements and finite element calculations. The apparent lattice parameters of both constrained phases are obtained in thin foils, using a new multi-pattern approach, which allows for unambiguous determination of all the lattice parameters considering the real symmetry of the strained crystals. Finite element calculations are used to establish relations between the constrained and unconstrained lattice parameters, with the stress relaxation resulting from the thin foil geometry taken into account. (C) 2011 Elsevier Ltd. All rights reserved.

Equipe: Département SI2M : Microstructures et Contraintes

Borgese, L., Gelfi, M., Bontempi, E., Goudeau, P., Geandier, G., Thiaudière, D. and Depero, L. E.
Surface and Coatings Technology, 206(8-9):2459-2463
2012
ISSN: 0257-8972

Resume: Atomic Layer Deposition (ALD) allows the deposition of thin films onto flat as well as complex geometry surfaces with excellent conformality. Thicknesses of few atomic layers can be achieved. Moreover, low-temperature deposition is possible and this enables the change of surface properties of many kinds of materials. Good adhesion characteristics and also good mechanical performance of ALD deposited thin films make the technique extremely interesting for several applications, as for example micro-electronics. TiO2 is a well studied semiconductor material because of its multifunctional properties that open a wide range of applications for example in photocatalysis, optics and solar cells. ALD is extremely completive to other technique, to deposit titania thin films, employed even to improve the biocompatibility of many kind of materials. TiO2 thin films are deposited with ALD technique at low temperature (90 degrees C) onto Kapton substrate and then crystallized ex-situ after annealing at 300 degrees C. X-ray diffraction (XRD) techniques are very suitable for the analysis of structure and microstructure of films and surface layers. In this work, XRD in combination with in situ tensile testing has been applied for the first time to measure elastic properties (elastic modulus and Poisson ratio) of TiO2 anatase thin films obtained by ALD. For the experimental conditions, the tensile stage was installed in a Synchrotron laboratory of Soleil. The information extracted from diffraction patterns is presented. (C) 2011 Elsevier B.V. All rights reserved.

Equipe: Département SI2M : Microstructures et Contraintes

2011

Articles:

Appolaire, Benoit, Perevoshchikova, Nataliya, Teixeira, Julien and Denis, Sabine
Solid State Phenomena, 172-174(Part 1):1214-1219
2011
ISSN: 1012-0394

Resume: We have adapted the Quickhull algorithm with the general dimension Beneath-Beyond algorithm [6] for computing the convex hull of the Gibbs energy hypersurface of multicomponent two-phase alloys. We illustrate the salient features of our method with calculations of isothermal ferrite-austenite equilibria in Fe-C-Cr. Finally, successive equilibrium calculations in a Fe-C-Cr-Mo steel over a large temperature range show the benefit of computing the convex hull before performing the conventional Newton-Raphson search.

Equipe: Département SI2M : Microstructures et Contraintes

Daoudi, M., Triki, A. and Redjaïmia, A.
Journal of Thermal Analysis and Calorimetry, 104 (2):627-633
2011

Equipe: Département SI2M : Microstructures et Contraintes

Borgese, L., Bontempi, E., Gelfi, M., Depero, L. E., Goudeau, P., Geandier, G. and Thiaudière, D.
Acta Materialia, 59(7):2891-2900
2011
ISSN: 1359-6454

Resume: Amorphous TiO2 thin films were deposited by means of atomic layer deposition on Kapton substrates and then crystallized ex situ by annealing at 300 degrees C to obtain the anatase phase. The morphology, structure and microstructure of films treated for 12, 24, 72 and 90 h were investigated. The local Ti coordination changes were studied by X-ray near-edge structure (XANES). On the basis of X-ray diffraction residual stress calculations, the elastic anisotropy of the films is experimentally determined for the first time (A*(comp) = 0.07, A*(shear) = 0.03). The film macro-strains increased with the time of treatment, while the micro-strains decreased. This effect may be correlated with the incipient anatase-to-rutile transformation as suggested by the changes observed in the XANES pattern of the film treated for 90 h. However, the contribution of the substrate cannot be excluded. (C) 2011 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Equipe: Département SI2M : Microstructures et Contraintes

2010

Articles:

Daoudi, Mourad Ibrahim, Triki, Abdelhafid and Redjaimia, Abdelkrim
Journal of Thermal Analysis and Calorimetry, 104(2):627-633
2010
ISSN: 1572-8943

Equipe: Département SI2M : Microstructures et Contraintes

Appolaire, Benoit, Aeby-Gautier, Elisabeth, Teixeira, Julien Da Costa, Dehmas, Moukrane and Denis, Sabine
Philisophical magazine, 90(1-4):461-483
2010
ISSN: 1478-6435

Resume: We propose a description of incoherent and semi-coherent interfaces within the framework of diffuse interface modelling: accounting for the discontinuity of tangential displacements is an issue addressed by introducing a new field, called the incoherency field, located in the diffuse interface and able to release the shear stresses tangential to the interface. After having demonstrated the ability of the model to recover trends obtained by sharp interface models of sliding interfaces, the process of loss of coherency is investigated by assuming a local process which would result from the competition between the shear stress release at the interface and the interfacial energy increase.

Equipe: Département SI2M : Microstructures et Contraintes

2008

Articles:

Daoudi, M.I., Triki, A. and Redjaïmia, A.
Algerian Journal of Advanced Materials, 5:13
2008

Equipe: Département SI2M : Microstructures et Contraintes

Bruneseaux, Fabien, Aeby-Gautier, Elisabeth, Geandier, Guillaume, Teixeira, Julien Da Costa, Appolaire, Benoit, Weisbecker, Patrick and Mauro, Anthony
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 476(1-2):60-68
2008
ISSN: 0921-5093

Resume: The beta(BCC) -> alpha(HCP) + beta(BCC) phase transformation kinetics of the beta-metastable titanium alloy Ti17 was studied by in situ high energy X-ray diffraction (XRD) and electrical resistivity. The use of synchrotron radiation (E = 89.12 keV, lambda = 0.01402 nm) allowed to characterize specimens 6 mm in diameter, limiting thus oxidation effects. The alpha + beta -> beta phase transformation kinetics was characterized during continuous heating up to the P temperature range. The beta -> alpha + beta transformation was studied in isothermal conditions (dwell at 708 degrees C or 750 degrees C) and during continuous cooling (cooling rates of 0.05 degrees C/s, 0.1 degrees C/s and 0.61 degrees C/s). The evolutions of the phase fractions are analyzed and compared to kinetics measured by electrical resistivity, showing a good correlation between both methods. In addition, the evolutions of the cell parameters of each phase obtained from XRD patterns are analyzed in regard of the transformation kinetics. (C) 2007 Elsevier B.V. All rights reserved.

Equipe: Département SI2M : Microstructures et Contraintes

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