[Article] Experimental design for nanoparticles synthesis by microwave

Abstract

The goal of this work is to determine the best microwave parameters of iron oxide nanoparticles synthesis for a better control of properties. An experimental design is performed to reduce the number of experiments from 1024 to 16 and a statistical approach is carried out to check the reproducibility and the repeatability of the synthesis. A simulation of these 1024 experiments is compared with random experiments.

Authors

Thomas Girardet, Morgane Kessler, Sylvie Migot, Lionel Aranda, Sébastien Diliberto, Stéphane Suire, Tom Ferté, Sébastien Hupont, Franck Cleymand, Solenne Fleutot

References

Thomas Girardet, Morgane Kessler, Sylvie Migot, Lionel Aranda, Sébastien Diliberto, Stéphane Suire, Tom Ferté, Sébastien Hupont, Franck Cleymand, Solenne Fleutot, One step superparamagnetic iron oxide nanoparticles by a microwave process: optimization of microwave parameters with an experimental design, Part. Part. Syst. Charact. 2024, 2300226

DOI

10.1002/ppsc.202300226